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[DOI] [PMC free article] [PubMed] [Google Scholar] 370.Sipula IJ, Brown NF, Perdomo G

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A 4-min-long linear gradient from 98% A (1% acetonitrile, 0.1% formic acid in water) to 90% B (0.1% formic acid in acetonitrile) at a flow rate of 100 µl/min has been used, employing a column temperature of 30 °C